1Mustafa Tareq Mahdi, 2Ali Aljalyf
1Physics nanotechnology / Osmania University
2Physics Solid state / Mazandaran U niversity
DOI : https://doi.org/10.47191/ijmra/v6-i10-47Google Scholar Download Pdf
ABSTRACT:
Silver nanoparticles (AgNPs) have been frequently studied in the scientific field due to their physical, chemical and biological properties. These characteristics are influenced by the nanomaterials' size, morphology and composition , allowing the application of AgNPs in the biomedical area due to their antimicrobial action. This work studied the influence of sodium citr ate concentration on the size of silver nanoparticles. Characterization techniques such as DLS and UV visible spectr oscopy were applied to analyze nanoparticle stability, size and polydispersity index. Characterization was carried out using a UV Vis Spectrophotometer and TEM (Transmission Electron Microscope). Analysis of the UV Vis spectra shows that the relatively sta ble nanoparticles at the maximum wavelength measurement of 417 to 418 nm are synthesized using 35, 55 and 100 mmol/L of sodium citrate. Characterization using TEM and XRD analysis shows that silver nanoparticles synthesized based on sodium citrate concentr ation have the smallest size in the 15.5 34.56 nm range with a face centred cubic (FCC) crystal structure. The nanoparticles utilized in this study demonstrated greater antimicrobial activity against Gram positive bacteria than Gram negative bacteria.
KEYWORD:Silver nanoparticles, characterization, sodium citrate, anti bacterial study
REFERENCES:1) Gandhi M, Amreen K. Emerging Trends in Nanomaterial-Based Biomedical Aspects. Electrochem. 2023; 4(3):365-388.
2) Harish V, Ansari MM, Tewari D, Gaur M, Yadav AB, García-Betancourt M-L, Abdel-Haleem FM, Bechelany M, Barhoum A. Nanoparticle and Nanostructure Synthesis and Controlled Growth Methods. Nanomaterials. 2022; 12(18):3226
3) Boughbina-Portolés A, Sanjuan-Navarro L, Moliner-Martínez Y, Campíns-Falcó P. Study of the Stability of Citrate Capped AgNPs in Several Environmental Water Matrices by Asymmetrical Flow Field Flow Fractionation. Nanomaterials. 2021; 11(4):926.
4) Sánchez-López E, Gomes D, Esteruelas G, Bonilla L, Lopez-Machado AL, Galindo R, Cano A, Espina M, Ettcheto M, Camins A, et al. Metal-Based Nanoparticles as Antimicrobial Agents: An Overview. Nanomaterials. 2020; 10(2):292.
5) La Spina R, Mehn D, Fumagalli F, Holland M, Reniero F, Rossi F, Gilliland D. Synthesis of Citrate-Stabilized Silver Nanoparticles Modified by Thermal and pH Preconditioned Tannic Acid. Nanomaterials. 2020; 10(10):2031.
6) Kim A, Ng WB, Bernt W, Cho NJ. Validation of Size Estimation of Nanoparticle Tracking Analysis on Polydisperse Macromolecule Assembly. Sci Rep. 2019 Feb 25;9(1):2639.
7) Lee P.C., Meisel D. Adsorption and Surface-Enhanced Raman of Dyes on Silver and Gold Sols. J. Phys. Chem. 1982;86:3391–3395.
8) Ingerslev F, Nyholm N. Shake-flask test for determination of biodegradation rates of (14)C-labeled chemicals at low concentrations in surface water systems. Ecotoxicol Environ Saf. 2000 Mar;45(3):274-83.
9) Jin H, Cai M, Deng F. Antioxidation Effect of Graphene Oxide on Silver Nanoparticles and Its Use in Antibacterial Applications. Polymers. 2023; 15(14):3045.
10) Giri, Anupam & Makhal, Abhinandan & Ghosh, Barnali & Raychaudhuri, Arup & Pal, Samir.Functionalization of manganite nanoparticles and their interaction with biologically relevant small ligands: Picosecond time-resolved FRET studies. Nanoscale. 2010: 2. 2704-9.
11) Xu L, Wang YY, Huang J, Chen CY, Wang ZX, Xie H. Silver nanoparticles: Synthesis, medical applications and biosafety. Theranostics. 2020 Jul 11;10(20):8996-9031.
12) Ranoszek-Soliwoda K, Tomaszewska E, Socha E, Krzyczmonik P, Ignaczak A, Orlowski P, Krzyzowska M, Celichowski G, Grobelny J. The role of tannic acid and sodium citrate in the synthesis of silver nanoparticles. J Nanopart Res. 2017;19(8):273.
13) Cobos M, De-La-Pinta I, Quindós G, Fernández MJ, Fernández MD. Graphene Oxide–Silver Nanoparticle Nanohybrids: Synthesis, Characterization, and Antimicrobial Properties. Nanomaterials. 2020; 10(2):376
14) Lee SH, Jun B-H. Silver Nanoparticles: Synthesis and Application for Nanomedicine. International Journal of Molecular Sciences. 2019; 20(4):865.
15) Salleh A, Naomi R, Utami ND, Mohammad AW, Mahmoudi E, Mustafa N, Fauzi MB. The Potential of Silver Nanoparticles for Antiviral and Antibacterial Applications: A Mechanism of Action. Nanomaterials. 2020; 10(8):1566.
16) Bruna T, Maldonado-Bravo F, Jara P, Caro N. Silver Nanoparticles and Their Antibacterial Applications. Int J Mol Sci. 2021 Jul 4;22(13):7202.
17) Zhang XF, Liu ZG, Shen W, Gurunathan S. Silver Nanoparticles: Synthesis, Characterization, Properties, Applications, and Therapeutic Approaches. Int J Mol Sci. 2016 Sep 13;17(9):1534
18) More PR, Pandit S, Filippis A, Franci G, Mijakovic I, Galdiero M. Silver Nanoparticles: Bactericidal and Mechanistic Approach against Drug Resistant Pathogens. Microorganisms. 2023 Feb 1;11(2):369.
19) Gouyau J, Duval RE, Boudier A, Lamouroux E. Investigation of Nanoparticle Metallic Core Antibacterial Activity: Gold and Silver Nanoparticles against Escherichia coli and Staphylococcus aureus. Int J Mol Sci. 2021 Feb 14;22(4):1905.
20) Yuan YG, Peng QL, Gurunathan S. Effects of Silver Nanoparticles on Multiple Drug-Resistant Strains of Staphylococcus aureus and Pseudomonas aeruginosa from Mastitis-Infected Goats: An Alternative Approach for Antimicrobial Therapy. Int J Mol Sci. 2017 Mar 6;18(3):569.
21) Liao C, Li Y, Tjong SC. Bactericidal and Cytotoxic Properties of Silver Nanoparticles. International Journal of Molecular Sciences. 2019; 20(2):449.
22) Ghodake G, Kim M, Sung JS, Shinde S, Yang J, Hwang K, Kim DY. Extracellular Synthesis and Characterization of Silver Nanoparticles-Antibacterial Activity against Multidrug-Resistant Bacterial Strains. Nanomaterials (Basel). 2020 Feb 19;10(2):360.
Volume 06 Issue 10 October 2023
There is an Open Access article, distributed under the term of the Creative Commons Attribution – Non Commercial 4.0 International (CC BY-NC 4.0) (https://creativecommons.org/licenses/by-nc/4.0/), which permits remixing, adapting and building upon the work for non-commercial use, provided the original work is properly cited.
Our Services and Policies
Authors should prepare their manuscripts according to the instructions given in the authors' guidelines. Manuscripts which do not conform to the format and style of the Journal may be returned to the authors for revision or rejected.
The Journal reserves the right to make any further formal changes and language corrections necessary in a manuscript accepted for publication so that it conforms to the formatting requirements of the Journal.
International Journal of Multidisciplinary Research and Analysis will publish 12 monthly online issues per year,IJMRA publishes articles as soon as the final copy-edited version is approved. IJMRA publishes articles and review papers of all subjects area.
Open access is a mechanism by which research outputs are distributed online, Hybrid open access journals, contain a mixture of open access articles and closed access articles.
International Journal of Multidisciplinary Research and Analysis initiate a call for research paper for Volume 07 Issue 12 (December 2024).
PUBLICATION DATES:
1) Last Date of Submission : 26 December 2024 .
2) Article published within a week.
3) Submit Article : editor@ijmra.in or Online
Why with us
1 : IJMRA only accepts original and high quality research and technical papers.
2 : Paper will publish immediately in current issue after registration.
3 : Authors can download their full papers at any time with digital certificate.
The Editors reserve the right to reject papers without sending them out for review.
Authors should prepare their manuscripts according to the instructions given in the authors' guidelines. Manuscripts which do not conform to the format and style of the Journal may be returned to the authors for revision or rejected. The Journal reserves the right to make any further formal changes and language corrections necessary in a manuscript accepted for publication so that it conforms to the formatting requirements of the Journal.